Chemical Tests

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test for hydrogen

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1

test for hydrogen

holding a burning splint held at the open end of a test tube of gas. If the gas is hydrogen it burns with a loud ‘squeaky pop’

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2

test for oxygen

If oxygen is present in a test tube, a glowing splint relights when it is held inside.

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3

test for carbon dioxide

If carbon dioxide is bubbled through limewater, the limewater turns milky or cloudy white

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4

test for chlorine

Damp litmus paper is bleached white when it is placed in chlorine.

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5

test for ammonia

Hold the litmus paper near the mouth of the test tube, damp red litmus paper turns blue

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6

how to carry out a flame test

  • Dip a clean wire loop into concentrated hydrochloric acid and heat to clean it. Then dip it in the hydrochloric acid again before dipping it into the metal compound that is being tested.

  • Hold the loop in the roaring bunsen burner flame

  • Use the colour of the flame to identify the metal compound.

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7

what color should the flame be and why

blue flame (open the collar so more oxygen can enter), so it will not contaminate the color of the flame

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8

what material should the wire be and why

nichrome or platinum as they have high melting point and do not contaminate the color

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9

lithium +

flame test red

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10

sodium +

flame test yellow / bright orange

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11

potassium +

flame test lilac

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12

calcium 2+

flame test red

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13

copper 2+ flame test

flame test blue-green

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14

NH4 + test

sodium hydroxide
warm the mixture
test for ammonia gas

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15

Cu 2+ non flame test

add sodium hydroxide Blue precipitate should form

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16

Fe 2+

add sodium hydroxide. green precipitate should form

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17

Fe 3+

Add sodium hydroxide brown precipitate should form

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18

Cl -

add nitric acid, add silver nitrate solution, white precipitate should form

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19

Br -

add nitric acid, add silver nitrate solution, cream precipitate should form

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20

I -

add nitric acid, add silver nitrate solution, yellow precipitate should form

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21

SO4 2-

add a few drops of barium nitrate solution should form a white precipitate

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22

CO3 2-

add hydrochloric acid and bubble through limewater, should turn cloudy

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23

water

add water to white anhydrous copper (II) sulfate and it turns blue

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24

pure water

Using a thermometer check if the boiling point is exactly 100 oC

Any impurities present will usually tend to raise the boiling point and depress the melting point of pure substance

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25

why do you add hydrochloric acid/ nitric acid in a negative ion test

To dissolve the compound and remove and carbonate ions, as they would also form a precipitate with the silver ions and so interfere with the test.

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26

what is limewater

calcium hydroxide

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